Fr. 176.00

Nanomaterial Characterization - An Introduction

Englisch · Fester Einband

Versand in der Regel in 3 bis 5 Wochen

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Informationen zum Autor Ratna Tantra is a Senior Scientist at National Physical Laboratory (NPL), UK. She has been at NPL for 14 years and worked on numerous projects in the field of nanoscience. Her multidisciplinary background was useful, allowing an expansion of her research portfolio in the area of nanomaterial characterization in different scientific disciplines, for example, surface-enhanced Raman spectroscopy and nanotoxicology. Before joining NPL, she was a research associate at Imperial College London, then University of Glasgow. She got her PhD in electrochemistry from University College London. She is a Chartered Scientist, Chartered Chemist, and member of the Royal Society of Chemistry. Klappentext * Introduces basic knowledge for nanomaterial characterization focusing on key properties and the different analytical techniques available* Provides a quick reference to different analytical methods for a given property highlighting their pros and cons* Presents numerous case studies, ranging from characterizing nanomaterials in coffee creamer suspension to measurement of airborne dust exposure levels* Provides an introduction to other topics that are strongly related to nanomaterial characterization e.g. synthesis, reference material and metrology* Includes state of the art techniques: scanning tunneling microscopy under extreme conditions, novel strategy for biological characterization and methods to visualize multidimensional characterization data Zusammenfassung * Introduces basic knowledge for nanomaterial characterization focusing on key properties and the different analytical techniques available* Provides a quick reference to different analytical methods for a given property highlighting their pros and cons* Presents numerous case studies! ranging from characterizing nanomaterials in coffee creamer suspension to measurement of airborne dust exposure levels* Provides an introduction to other topics that are strongly related to nanomaterial characterization e.g. synthesis! reference material and metrology* Includes state of the art techniques: scanning tunneling microscopy under extreme conditions! novel strategy for biological characterization and methods to visualize multidimensional characterization data Inhaltsverzeichnis List of Contributors xv Editor's Preface xix 1 Introduction 1 1.1 Overview 1 1.2 Properties Unique to Nanomaterials 3 1.3 Terminology 4 1.3.1 Nanomaterials 4 1.3.2 Physicochemical Properties 7 1.4 Measurement of Good Practice 8 1.4.1 Method Validation 8 1.4.2 Standard Documents 13 1.5 Typical Methods 16 1.5.1 Sampling 16 1.5.2 Dispersion 19 1.6 Potential Errors Due to Chosen Methods 20 1.7 Summary 20 Acknowledgments 21 References 21 2 Nanomaterial Syntheses 25 2.1 Introduction 25 2.2 Bottom-Up Approach 26 2.2.1 Arc-Discharge 26 2.2.2 Inert-Gas Condensation 26 2.2.3 Flame Synthesis 27 2.2.4 Vapor-Phase Deposition 27 2.2.5 Colloidal Synthesis 27 2.2.6 Biologically synthesized nanomaterials 28 2.2.7 Microemulsion Synthesis 28 2.2.8 Sol-Gel Method 29 2.3 Synthesis: Top-Down Approach 29 2.3.1 Mechanical Milling 29 2.3.2 Laser Ablation 30 2.4 Bottom-Up and Top-Down: Lithography 30 2.5 Bottom-Up or Top-Down? Case Example: Carbon Nanotubes (CNTs) 30 2.6 Particle Growth: Theoretical Considerations 32 2.6.1 Nucleation 32 2.6.2 Particle Growth and Growth Kinetics 33 2.6.2.1 Diffusion-Limited Growth 33 2.6.2.2 Ostwald Ripening 34 2.7 Case Study: Microreactor for the Synthesis of Gold Nanoparticles 34 2.7.1 Introduction 34 2.7.2 Method 36 2.7.2.1 Materials 36 2.7.2.2 Protocol: Nanoparticles Batch Synthesis 37 2.7.2....

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