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Filling a gap in the literature, this timely publication is the first to comprehensively cover the emerging and rapidly growing field of the synthesis of nanoparticles using microwaves. Divided into the three parts of fundamentals, methods and applications, the handbook presents such hot topics as microwave theory, scale-up, microwave plasma synthesis, characterization and much more. With its excellent and experienced editor team, this book is of high interest to those working in industry due to the number of possible applications in semiconductors,electronics, catalysis, and sensors, to name but a few examples.
Sommario
PREFACE INTRODUCTION TO NANOPARTICLES General Introduction to NanoparticlesMethods of Nanoparticle Synthesis Surface Plasmon Resonance and Coloring Control of Size, Shape, and Structure Reducing Agent in Nanoparticle Synthesis Applications of Metallic Nanoparticles GENERAL FEATURES OF MICROWAVE CHEMISTRY Microwave Heating Some Applications of Microwave Heating Microwave Chemistry Microwave Chemical Reaction Equipment CONSIDERATIONS OF MICROWAVE HEATING General Considerations of Microwave Heating Peculiar Microwave Heating Relevant Points of Effective Microwave Heating COMBINED ENERGY SOURCES IN THE SYNTHESIS OF NANOMATERIALS Introduction Simultaneous Ultrasound/Microwave Treatments Sequential Ultrasound and Microwaves Conclusions NANOPARTICLE SYNTHESIS THROUGH MICROWAVE HEATING Introduction Microwave Frequency Effects Nanoparticle Synthesis under a Microwave Magnetic Field Synthesis of Metal Nanoparticles by a Greener Microwave Hydrothermal Method Nanoparticle Synthesis with Microwaves under Cooling Conditions Positive Aspects of Microwaves - Thermal Distribution in Nanoparticle Synthesis Microwave-Assisted Nanoparticle Synthesis in Continuous Flow Apparatuses MICROWAVE-ASSISTED SOLUTION SYNTHESIS OF NANOMATERIALS Introduction Synthesis of ZnO Nanocrystals Synthesis of a-Fe2O3 Nanostructures Element-Based Nanostructures and Nanocomposite Chalcogenide Nanostructures Graphene Summary PRECISELY CONTROLLED SYNTHESIS OF METAL NANOPARTICLES UNDER MICROWAVEIRRADIATION Introduction Precise Control of Single Component under Microwave Irradiation Precise Control of Multicomponent Structures under Microwave IrradiationAn Example of Mass Production Oriented to Application Conclusion MICROWAVE-ASSISTED NONAQUEOUS ROUTES TO METAL OXIDE NANOPARTICLESAND NANOSTRUCTURES Introduction Nonaqueous Sol - Gel Chemistry Polyol Route Benzyl Alcohol Route Other Mono-Alcohols Ionic Liquids Nonaqueous Microwave Chemistry beyond Metal Oxides Summary and Outlook INPUT OF MICROWAVES FOR NANOCRYSTAL SYNTHESIS AND SURFACEFUNCTIONALIZATION FOCUS ON IRON OXIDE NANOPARTICLES Introduction Biomedical Applications of Iron Oxide Nanoparticles Nanoparticle Synthesis Nanoparticle Surface Functionalization Microwave-Assisted ChemistryConclusions MICROWAVE-ASSISTED CONTINUOUS SYNTHESIS OF INORGANIC NANOMATERIALS Introduction and Overview Microwave-Assisted Continuous Synthesis of Inorganic Nanomaterials Types of Microwave Apparatus Used in Continuous SynthesisMicrowave Continuous Synthesis of Molecular Sieve MaterialsMicrowave Continuous Synthesis of Metal Oxides and Mixed Metal Oxide Materials Microwave Continuous Synthesis of Metallic Nanomaterials Conclusions and Outlook MICROWAVE PLASMA SYNTHESIS OF NANOPARTICLES: FROM THEORETICAL BACKGROUND AND EXPERIMENTAL REALIZATION TO NANOPARTICLES WITH SPECIAL PROPERTIES Introduction Using Microwave Plasmas for Nanoparticle Synthesis Experimental Realization of the Microwave Plasma Synthesis Infl uence of Experimental Parameters Nanoparticle Properties and Application Summary OXIDATION, PURIFI CATION AND FUNCTIONALIZATION OF CARBON NANOTUBES UNDERMICROWAVE IRRADIATION Introduction Oxidation and Purifi cationFunctionalization Conclusion INDEX
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Nick Serpone is Professor Emeritus and Visiting Professor at the University of Pavia, Italy. As a senior academic and research scientist in organic and photochemistry, program manager and industry consultant with extensive North American and international experience, he has an intimate knowledge of the working relationships between academia, industry and government agencies in various countries. Nick Serpone is a prolific editor and contributor to numerous books and journals, with over 360 papers published in a variety of prestigious journals. Nick Serpone is a frequent Keynote Address Speaker and Invited Plenary Lecturer.
Riassunto
Filling a gap in the literature, this timely publication is the first to comprehensively cover the emerging and rapidly growing field of the synthesis of nanoparticles using microwaves. Divided into the three parts of fundamentals, methods and applications, the handbook presents such hot topics as microwave theory, scale-up, microwave plasma synthesis, characterization and much more. With its excellent and experienced editor team, this book is of high interest to those working in industry due to the number of possible applications in semiconductors,
electronics, catalysis, and sensors, to name but a few examples.
