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Ein Klassiker und Beststeller, jetzt in vierter Auflage! Gut lesbar und ohne weitschweifige Exkurse behandelt das Werk alle Aspekte der Ionenchromatographie. Neu hinzugekommen sind Informationen zur Kapillarelektrophorese, zu monolithischen Säulen und Mikromethoden; die theoretischen Grundlagen der IC werden jetzt ausführlich behandelt. Übersichtliche Tabellen zu Detektionsverfahren, Elutionsbedingungen und anderen Themen runden den praxistauglichen Text ab.
List of contents
INTRODUCTION AND OVERVIEWIntroductionHistorical DevelopmentPrinciples of Ion Chromatographic Separation and DetectionINSTRUMENTATIONComponents of an Ion Chromatograph (IC) InstrumentGeneral ConsiderationsEluentPumpSample InjectorColumnsSuppressorDetectorData Acquisition and Calculation of ResultsRESINS AND COLUMNSIntroductionPolymeric ResinsResins and Columns for Ion ChromatographyAnion ExchangersCation ExchangersOther ResinsDETECTORSIntroductionConductivity DetectorsUltraviolet-Visible (UV-Vis) DetectorsFluorescence DetectorElectrochemical DetectorsRefractive Index DetectorEvaporative Light Scattering Detector (ELSD)Other DetectorsPRINCIPLES OF ION CHROMATOGRAPHIC SEPARATIONSGeneral ConsiderationsChromatographic TermsSelectivityChromatographic EfficiencyANION CHROMATOGRAPHYScope and Conditions for SeparationSuppressed Anion ChromatographyNonsuppressed Ion ChromatographyCoated ColumnsOptical Absorbance DetectionDetectionPulsed Amperometric Detector (PAD)Evaporative Light Scattering Detector (ELSD)Inductively Coupled Plasma Methods (ICP)CATION CHROMATOGRAPHYIntroductionColumnsSeparationsEffect of Organic SolventsSeparation of Metal Ions with a Complexing EluentChelating Ion-Exchange Resins and Chelation Ion ChromatographyION-EXCLUSION CHROMATOGRAPHYPrinciplesSeparation of Organic AcidsSimultaneous Determination of Anions and CationsConclusionsDetermination of Carbon Dioxide and BicarbonateSeparation of BasesDetermination of WaterSeparation of Saccharides and AlcoholsION PAIR CHROMATOGRAPHYPrinciplesTypical SeparationsMechanismZWITTERION STATIONARY PHASESIntroductionSimultaneous Separation of Anions and CationsSeparation of AnionsSeparation of CationsMechanismCAPILLARY ELECTROPHORESISIntroductionPrinciplesElectroosmotic Flow (EOF)Separations of IonsCapillary Electrophoretic Ion ChromatographyDNA AND RNA CHROMATOGRAPHYIntroductionDNA and RNA Chemical Structure and PropertiesDNA and RNA ChromatographyTemperature Modes of DNA and RNA ChromatographyInstrumentationApplications of DNA ChromatographyApplications of RNA ChromatographySAMPLE PRETREATMENTDilute and Shoot or Pre-Treat the Sample?Particulate and Column-Contaminating MatterPreconcentrationSample PretreatmentMETHOD DEVELOPMENT AND VALIDATIONChoosing a MethodSome Applications of Ion ChromatographyStatistical Evaluation of DataValidation of Analytical ProceduresCHEMICAL SPECIATIONIntroductionDetectionChromatographyValveless Injection ICSpeciation of Some Elements
About the author
After having obtained his Ph.D. in 1948 by the University of Illinois, Prof. James S. Fritz became Senior Chemist and Professor of Chemistry at Iowa State University in 1960 where he became Distinguished Professor in Liberal Arts and Sciences in 1990. Besides Ion Chromatography his research interests are titrations, solid-phase extractions, capillary electrophoresis and analytical complexing reagents.
Douglas T. Gjerde received his PhD in analytical chemistry from Iowa State University. After having worked in large and small companies for a number of years, Gjerde founded Sarasep, Inc. in 1990 for the commercialization of polymeric separation technologies and co-founded Transgenomic, Inc. in 1997 for the commercialization of nucleic acid separation technology. Gjerde is now working on his third start-up company, PhyNexus, Inc. PhyNexus produces miniaturized sample preparation tools for the biological research market. Gjerde has authored and coauthored numerous articles, book chapters and several books and holds over fifty patents in separation science.
Summary
Ein Klassiker und Beststeller, jetzt in vierter Auflage! Gut lesbar und ohne weitschweifige Exkurse behandelt das Werk alle Aspekte der Ionenchromatographie. Neu hinzugekommen sind Informationen zur Kapillarelektrophorese, zu monolithischen Säulen und Mikromethoden; die theoretischen Grundlagen der IC werden jetzt ausführlich behandelt. Übersichtliche Tabellen zu Detektionsverfahren, Elutionsbedingungen und anderen Themen runden den praxistauglichen Text ab.
Report
"Overall, this is a good book for those interested in the separation of small inorganic and organic ions. It takes the reader from beginner to intermediate level in terms of the understanding and practice of ion chromatography. It is an easy to read book and for those wishing to build up their knowledge of the topic quickly, it is strongly recommended." (Chromatographia, August 2010)
"This new edition is a substantial expansion and update of the previous edition, and is strongly recommended for scientists seeking a broad overview of IC. I am sure that this fourth edition will continue the success of its predecessors." ( Analytical and Bioanalytical Chemistry , Jan - June 2010)
