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Informationen zum Autor Philippa B. Cranwell, PhD is a Lecturer in the Department of Chemistry, University of Reading, UK. Laurence M. Harwood, PhD is Professor of Organic Chemistry in the Department of Chemistry and Director of the Chemical Analysis Facility, University of Reading, UK. Christopher J. Moody, PhD is Sir Jesse Boot Professor in the School of Chemistry, University of Nottingham, UK. Klappentext The definitive guide to the principles and practice of experimental organic chemistry - fully updated and now featuring more than 100 experiments The latest edition of this popular guide to experimental organic chemistry takes students from their first day in the laboratory right through to complex research procedures. All sections have been updated to reflect new techniques, equipment and technologies, and the text has been revised with an even sharper focus on practical skills and procedures. The first half of the book is devoted to safe laboratory practice as well as purification and analytical techniques; particularly spectroscopic analysis. The second half contains step-by-step experimental procedures, each one illustrating a basic principle, or important reaction type. Tried and tested over almost three decades, over 100 validated experiments are graded according to their complexity and all are chosen to highlight important chemical transformations and to teach key experimental skills. New sections cover updated health and safety guidelines, additional spectroscopic techniques, electronic notebooks and record keeping, and techniques, such as semi-automated chromatography and enabling technologies such as the use of microwave and flow chemistry. New experiments include transition metal-catalysed cross-coupling, organocatalysis, asymmetric synthesis, flow chemistry, and microwave-assisted synthesis. Key aspects of this third edition include: ¿ Detailed descriptions of the correct use of common apparatus used in the organic laboratory ¿ Outlines of practical skills that all chemistry students must learn ¿ Highlights of aspects of health and safety in the laboratory, both in the first section and throughout the experimental procedures ¿ Four new sections reflecting advances in techniques and technologies, from electronic databases and information retrieval to semi-automated chromatography ¿ More than 100 validated experiments of graded complexity from introductory to research level ¿ A user-friendly experiment directory ¿ An instructor manual and PowerPoint slides of the figures in the book available on a companion website A comprehensive guide to contemporary organic chemistry laboratory principles, procedures, protocols, tools and techniques, Experimental Organic Chemistry, Third Edition is both an essential laboratory textbook for students of chemistry at all levels, and a handy bench reference for experienced chemists. Zusammenfassung The definitive guide to the principles and practice of experimental organic chemistry - fully updated and now featuring more than 100 experiments The latest edition of this popular guide to experimental organic chemistry takes students from their first day in the laboratory right through to complex research procedures. Inhaltsverzeichnis About the authors ix Preface to the third edition xi About the companion website xv Part 1: Laboratory Practice 1 1 Safety in the chemical laboratory 3 1.1 Essential rules for laboratory safety 4 1.2 Hazardous chemicals 7 1.3 Disposal of hazardous waste 11 1.4 Accident procedures 12 2 Glassware and equipment in the laboratory 15 2.1 Glass equipment 16 2.2 Hardware 21 2.3 Heating 24 2.4 Stirring 30 2.5 Vacuum pumps 32 2.6 The rotary evaporator 42 2.7 Catalytic hydr...
