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Informationen zum Autor Rajmund Michalski works at the Institute of Environmental Engineering of Polish Academy of Sciences. He has authored/edited a dozen of books and over 250 publications about applications of ion chromatography in environmental samples analysis, as well as application of modern analytical methods and techniques for environmental protection and assessment. Since 2005 he has annually organized the since international ion chromatography conference in Poland. Klappentext Introduces the reader to the field of ion chromatography, species analysis and hyphenated methods IC-MS and IC-ICP-MS including the theory and theirs applications* Covers the importance of species analysis and hyphenated methods in ion chromatography* Includes practical applications of IC-MS and IC-ICP-MS in environmental analysis* Details sample preparation methods for ion chromatography* Discusses hyphenated methods IC-MS and IC-ICP-MS used in determining both the total element contents and its elements* Details speciation analysis used in studying biochemical cycles of selected chemical compounds; determining toxicity and ecotoxicity of elements; food and pharmaceuticals quality control; and in technological process control and clinical analytics Zusammenfassung Introduces the reader to the field of ion chromatography! species analysis and hyphenated methods IC-MS and IC-ICP-MS including the theory and theirs applications* Covers the importance of species analysis and hyphenated methods in ion chromatography* Includes practical applications of IC-MS and IC-ICP-MS in environmental analysis* Details sample preparation methods for ion chromatography* Discusses hyphenated methods IC-MS and IC-ICP-MS used in determining both the total element contents and its elements* Details speciation analysis used in studying biochemical cycles of selected chemical compounds; determining toxicity and ecotoxicity of elements; food and pharmaceuticals quality control; and in technological process control and clinical analytics Inhaltsverzeichnis List of Contributors ix Preface xi 1 Principles and Applications of Ion Chromatography 1 Rajmund Michalski 1.1 Principles of Ion Chromatography, 1 1.1.1 Introduction, 1 1.1.2 Stationary Phases, 6 1.1.3 Eluents, 13 1.1.4 Suppressors, 16 1.1.5 Detection Methods, 18 1.2 Ion Chromatography Applications, 23 1.2.1 Speciation Analysis with the Hyphenated Methods of IC-ICP-MS and IC-MS, 29 1.3 Sample Preparation for Ion Chromatography, 32 1.4 Selected Methodological Aspects of Ion Determination with Ion Chromatography, 34 1.5 Ion Chromatography Development Perspectives, 37 1.6 References, 37 2 Mass Spectrometric Detectors for Environmental Studies 47 Maria Balcerzak 2.1 Introduction, 47 2.2 Mass Spectrometric Detectors, 49 2.2.1 Ionization Methods, 50 2.2.2 Mass Analyzers, 58 Acknowledgments, 62 2.3 References, 62 3 High-Performance Liquid Chromatography Coupled to Inductively Coupled Plasma MS/Electrospray Ionization MS 79 Jürgen Mattusch 3.1 Separation Principles, 79 3.1.1 Ion Chromatography (Anion/Cation Exchange, Mixed Mode), 80 3.1.2 High-Performance Liquid Chromatography (Reversed-Phase Mode, HILIC), 81 3.1.3 Size Exclusion Chromatography (SEC) (Gel Filtration Chromatography, GFC), 82 3.2 Detection Principles, 83 3.2.1 Common Detection in IC: Conductivity, UV-Vis, Electrochemical Detection, 83 3.2.2 Element Specific Detection, 83 3.3 Hyphenated Techniques, 87 3.3.1 HPLC(IC)-ICP-MS, 87 3.4 HPLC(IC)-ICP-MS/ESI-MS, 90 3.4.1 Fundamentals, 90 3.4.2 Methodology of Data Evaluation, 90 3.4.3 Technical Requirements, 91 3.5 Applications and Conclusion, 91 <...
