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Mit Ultraschall kann man den Fortgang von Reaktionen verfolgen und Arbeitsschritte in der Analytik beschleunigen. Neben den klassischen Anwendungen in der Extraktion stellt dieser Band auch moderne Einsatzgebiete, unter anderem in der Proteomforschung und Polymertechnik, vor. Spezielle Kapitel widmen sich den erforderlichen Instrumenten wie Ultraschallbädern und -sonden.
List of contents
THE POWER OF ULTRASOUND
Introduction
Cavitation
Common Ultrasonic Devices Used in Analytical Chemistry
Current Ultrasonic Devices for New Analytical Applications
ULTRASONIC ENERGY AS A TOOL FOR SAMPLE TREATMENT FOR THE ANALYSIS OF ELEMENTS AND ELEMENTAL SPECIATION
Introduction
Parameters Influencing Element Ultrasonic Solid-Liquid Extraction
US-SLE from Soils and Sediments
US-SLE from Sewage Sludge
US-SLE Extraction from Plants
Extraction from Soft Tissues
Total Element Determination
Elemental Fractionation and Elemental Speciation
On-Line Applications
Current Trends
ULTRASONIC ASSISTED EXTRACTION FOR THE ANALYSIS OF ORGANIC COMPOUNDS BY CHROMATOGRAPHIC TECHNIQUES
Introduction
Overview of Classic and Modern Extraction Procedures for Organics
Ultrasonic Assisted Extraction (UAE)
Coupling Ultrasound with Other Extraction Techniques
Comparison between UAE and Other Extraction Techniques
ELECTROCHEMICAL APPLICATIONS OF POWER ULTRASOUND
Introduction
Electrochemical Cell and Experimental Setup
Voltammetry Under Insonation
Trace Detection by Stripping Voltammetry
Biphasic Sonoelectroanalysis
Microelectrodes an Ultrasound
POWER ULTRASOUND MEETS PROTEOMICS
Introduction
Protein Identification Through Mass-Based Spectrometry Techniques and Peptide Mass Fingerprint
Classic In-Gel Protein Sample Treatment for Protein Identification Through Peptide Mass Fingerprint
Ultrasonic Energy for the Acceleration on In-Gel Protein Sample Treatment for Protein Identification Through Peptide Mass Fingerprint
Classic In-Solution Protein Sample Treatment for Protein Identification Through Peptide Mass Fingerprint
Ultrasonic Energy for the Acceleration of the In-Solution Protein Sample Treatment for Protein Identification Through Peptide Mass Fingerprint
BEYOND ANALYTICAL CHEMISTRY
Introduction
Sonochemistry for Organic Synthesis
Ultrasonic Enhanced Synthesis of Inorganic Nanomaterials
Sonochemistry Applied to Polymer Science
About the author
J. L. Capelo-Martínez obtained his PhD in chemistry in 2002 from the University of Vigo, Spain, where he was associate professor from 1999 to 2002. In December 2004 he became Research Fellow at the Associated Laboratory REQUIMTE, as well as at the Chemistry Department of the New University of Lisbon, and in 2006 was invited as an auxiliary professor to the same institution. His research work is related to new uses of ultrasonic energy as a tool at the Analytical Chemistry Laboratory. Dr. Capelo has more than fifty manuscripts and several patents to his name, he is a regular referee for various analytical journals and a member of the advisory board of the Analytical Journal TALANTA.
Summary
Mit Ultraschall kann man den Fortgang von Reaktionen verfolgen und Arbeitsschritte in der Analytik beschleunigen. Neben den klassischen Anwendungen in der Extraktion stellt dieser Band auch moderne Einsatzgebiete, unter anderem in der Proteomforschung und Polymertechnik, vor. Spezielle Kapitel widmen sich den erforderlichen Instrumenten wie Ultraschallbädern und -sonden.
Report
" The book can be recommended to practicing analytical chemists who need to develop more efficient strategies for analysis, and in general to those practitioners who need to improve analytical methodological performance. It could also serve as a valuable starting point for researching new avenues in the analytical use of ultrasound ." (Anal Bioanal Chem, 2009)
"Analytical Applications is a practical book that emphasizes some of the latest developments in the implementation of ultrasound in the analytical lab." ( Analytical and Bioanalytical Chemistry , August 2009)
