Analytical Methods in Supramolecular Chemistry, 2 Vols.

The second edition of "Analytical Methods in Supramolecular Chemistry" comes in two volumes and covers a broad range of modern methods and techniques now used for investigating supramolecular systems, e. g. NMR spectroscopy, mass spectrometry, extraction methods, crystallography, single molecule spectroscopy, electrochemisty, and many more. In this second edition, tutorial inserts have been introduced, making the book also suitable as supplementary reading for courses on supramolecular chemistry. All chapters have been revised and updated and four new chapters have been added.A must-have handbook for Organic and Analytical Chemists, Spectroscopists, Materials Scientists, and Ph.D. Students in Chemistry.From reviews of the first edition:"This timely book should have its place in laboratories dealing with supramolecular objects. It will be a source of reference for graduatestudents and more experienced researchers and could induce new ideas on the use of techniques other than those usually used in the laboratory."Journal of the American Chemical Society (2008) VOL. 130, NO. 1 doi: 10.1021/ja0769649"The book as a whole or single chapters will stimulate the reader to widen his horizon in chemistry and will help him to have new ideas in his research."Anal Bioanal Chem (2007) 389:2039-2040 DOI: 10.1007/s00216-007-1677-1

List of contents

PrefaceVolume OneINTRODUCTIONSome Historical Remarks on Supramolecular ChemistryThe Noncovalent Bond: a Brief OverviewBasic Concepts in Supramolecular ChemistryConclusions: Diverse Methods for a Diverse Research AreaQUANTITATIVE ANALYSIS OF BINDING PROPERTIESTheoretical PrinciplesA Practical Course of Binding Constant Determination by UV/Vis SpectroscopyPractical Course of Action for NMR Spectroscopic Binding Constant DeterminationOther Important Examples with Practical Actions of Data TreatmentConclusionISOTHERMAL TITRATION CALORIMETRY IN SUPRAMOLECULAR CHEMISTRYIntroductionThe Thermodynamic PlatformAcquiring Experimental Calorimetric DataExtending the Measurement RangePerspectivesEXTRACTION METHODSIntroductionThe Extraction TechniqueThe Technical ProcessThe Extraction EquilibriumPrinciples of Supramolecular ExtractionExamples of Supramolecular ExtractionConclusions and Future PerspectivesMASS SPECTROMETRY AND GAS PHASE CHEMISTRY OF SUPRAMOLECULESIntroductionInstrumentationParticularities and Limitations of Mass SpectrometryBeyond Analytical Characterization: Tandem MS Experiments for the Examination of the Gas-Phase Chemistry of SupramoleculesSelected ExamplesConclusionsDIFFUSION NMR IN SUPRAMOLECULAR CHEMISTRY AND COMPLEXED SYSTEMSIntroductionConcepts of Molecular DiffusionMeasuring Diffusion with NMRApplications of Diffusion NMR in Supramolecular Chemistry: Selected ExamplesAdvantages and Limitations of High Resolution Diffusion NMRDiffusion NMR and Chemical ExchangeDiffusion Modes and Signal Decay in Diffusion MR ExperimentsApplications of Diffusion NMR in Complex SystemsSummary and OutlookPHOTOPHYSICS AND PHOTOCHEMISTRY OF SUPRAMOLECULAR SYSTEMSIntroductionSpectrophotometry and SpectrofluorometryTime-Resolved Fluorescence TechniquesFluorescence AnisotropyTransient Absorption SpectroscopyConcluding RemarksCIRCULAR DICHROISM SPECTROSCOPYBasic ConsiderationsMeasurement Techniques (Methodology of CD Measurement)Processing of Circular Dichroism SpectraTheoryExamples of Vibrational Circular Dichroism ApplicationsConcluding RemarksVolume TwoELECTROCHEMICAL METHODSIntroductionBasic Principles of ElectrochemistryOverview of Electrochemical TechniquesElectrochemical Analysis of Supramolecular SystemsSelected ExamplesConcluding RemarksCRYSTALLOGRAPHY AND CRYSTAL ENGINEERING IntroductionCrystallographyCrystal EngineeringMethyl-Resorcinarene as a Crystal Engineering TargetConcluding RemarksSCANNING PROBE MICROSCOPYIntroduction: What Is the Strength of Scanning Probe Techniques?How Do Scanning Probe Microscopes Work?Which Molecules Can Be Studied?What Results Have Been Obtained in the Field of Supramolecular Chemistry?SINGLE-MOLECULE FORCE SPECTROSCOPY OF SUPRAMOLECULAR COMPLEXESIntroduction and MotivationFunctionally Immobilizing SupramoleculesSupramolecular Interactions Investigated by AFM-SMFSSummary and OutlookCONFOCAL LASER SCANNING MICROSCOPY: A VERSATILE SPECTROSCOPIC TOOL FOR THE INVESTIGATION OF MOLECULAR GELSIntroduction: Molecular GelsMethods Classically Used for the Characterization of Molecular GelsConfocal Laser Scanning Microscopy (CLSM)ConclusionTRANSMISSION ELECTRON MICROSCOPY (TEM) OF RADIATION SENSITIVE SUPRAMOLECULAR ARCHITECTURES - STRATEGIES FOR A COMPREHENSIVE STRUCTURE CHARACTERIZATIONIntroductionInstrumentationContrast in TEMSample PreparationStrategies and Examples to Characterize Supramolecular Structures by Complementary TEM MethodsTHE CHARACTERIZATION OF SYNTHETIC ION CHANNELS AND PORESIntroductionMethodsCharacteristicsStructural StudiesConcluding RemarksTHEORETICAL METHODS FOR SUPRAMOLECULAR CHEMISTRYIntroductionA Survey of Theoretical MethodsStandard Classification of Intermolecular InteractionsQualitative Understanding and Decomposition SchemesGeneral Mechanism for a Static, Step-Wise View on Host-Guest RecognitionConclusions and PerspectiveIndex

About the author

Christoph Schalley has received his PhD under the guidance of Helmut Schwarz and did his postdoctorate with Julius Rebek at the Scripps Research Institute in California. Currently, he is assistant professor in Bonn and has already authored more than 85 publications and four books. He was awarded with the Dozentenstipendium in 2004 of the Fonds der Chemischen Industrie.

Summary

The second edition of "Analytical Methods in Supramolecular Chemistry" comes in two volumes and covers a broad range of modern methods and techniques now used for investigating supramolecular systems, e. g. NMR spectroscopy, mass spectrometry, extraction methods, crystallography, single molecule spectroscopy, electrochemisty, and many more. In this second edition, tutorial inserts have been introduced, making the book also suitable as supplementary reading for courses on supramolecular chemistry. All chapters have been revised and updated and four new chapters have been added.

A must-have handbook for Organic and Analytical Chemists, Spectroscopists, Materials Scientists, and Ph.D. Students in Chemistry.

From reviews of the first edition:

"This timely book should have its place in laboratories dealing with supramolecular objects. It will be a source of reference for graduate
students and more experienced researchers and could induce new ideas on the use of techniques other than those usually used in the laboratory."
Journal of the American Chemical Society (2008) VOL. 130, NO. 1 doi: 10.1021/ja0769649

"The book as a whole or single chapters will stimulate the reader to widen his horizon in chemistry and will help him to have new ideas in his research."
Anal Bioanal Chem (2007) 389:2039-2040 DOI: 10.1007/s00216-007-1677-1

Product details

• Authors: Christoph A. Schalley
• Assisted by: Christop A Schalley (Editor), Christoph A Schalley (Editor), Christoph Schalley (Editor), Christoph A. Schalley (Editor)
• Publisher: Wiley-VCH
• Languages: English
• Product format: Mixed media product
• Released: 01.03.2012
• EAN: 9783527329823
• ISBN: 978-3-527-32982-3
• No. of pages: 808
• Weight: 1900 g
• Illustrations: 312 SW-Abb., 56 Farbabb., 19 Tabellen
• Subjects: Natural sciences, medicine, IT, technology > Chemistry > Organic chemistry; Chemie, Nanotechnologie, Analytische Chemie, Spektroskopie, chemistry, SUPRAMOLECULAR CHEMISTRY, supramolekulare Chemie, spectroscopy, Nanotechnology, Nanochemistry, Analytical Chemistry, Nanochemie